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Toxics Use Reduction Institute · Surface Solutions Laboratory
 
Toxics Use Reduction Institute




Surface Solutions Laboratory

Trial Report



Trial Number 3

(Client Number 244, Project Number 1)

Trial Purpose: To evaluate impact resistance for various floor finishes

Date Run: 06/03/05

Experiment Procedure:
The moisture content at the time of testing will influence results due to the hydroscopic nature of the base materials. Therefore, efforts must be taken to ensure that the moisture content and temperature remain constant during the evaluation period. Ideally, the sample floor should be kept at 65+/-1% relative humidity and 68+/-6 F.

During laboratory testing, conditions were slightly drier, 40% relative humidity, but the temperature was within the given temperature range ~70 F).

Sample Preparation
The flooring material supplied was Hardwood flooring made from Red Oak. The boards were ?? thick, 2 ?? wide and cut into 8? sections. Some pieces of the flooring had to be sanded prior to making initial thickness readings to remove residual packing tape adhesive. With the boards cut into 8? coupons, three readings were made using a Brown & Sharpe Micrometer to measure each coupons initial board thickness. Each reading was made to 0.001? and the three values were averaged to give a baseline thickness for the coupons. In addition to the thickness baseline, baselines were established for Gloss, Coefficient of Friction, Impact, Small Area Loads. Procedures for each baseline measurements followed the procedures to be outlined.

Following the establishment of the baselines, three coupons were coated with a supplied floor finish according to the manufacturers? specifications. The finish was applied using a 1? Pure Bristle 1500 paint brush. To ensure consistent coating application, the finish was leveled off using a 10 mils Precision Gage & Tool Co Dow Film Caster. Three coats were used for each floor finish as this was common number of coating layers suggested by the various manufacturers. Each coating layer was allowed to dry for 2 hours prior to the application of the next coat. Completed coupons were allowed to sit for a minimum period of 24 hours before performance evaluations were conducted.

Falling-Ball Indentation
This test is designed to obtain a measure of the resistance of a flooring finish to impacts from dropped objects. Four drops were made for each coupon for a total of twelve drops per finish. Each drop was made at a 6? intervals starting at 6? and ending at 72?. The ball used for the drops was a 440-C stainless steel 2? diameter ball, grade 100. The dropping apparatus used is shown in Figure 2. Carbon paper was placed on the coupon surface to assist in determining where the indentation was made.

Figure 2. Dropping Apparatus

The same Brown & Sharpe Micrometer was used to measure the indentations to the coated coupons. A plot was made of the height of drop and residual indentation and the slope of the best fit line was calculated. From the plots, the intercept of the height of drop at 72? was recorded as the index of indentation resistance. Results for each finish were compared each other.

Trial Results
Impact depth was calculated by subtracting the average initial coating thickness from the thickness measured at the point of impact for each drop
height. The initial average coating thickness was calculated from the three initial coating measurements made for each coupon.

Measured Thickness
      Coated Thickness         Drop Height                                 
Prod Coupon  Mid   End 1 End 2 6     12    18    24    30    36    42    48  54   60    66    72
2      22    7.506 7.506 7.502 7.503       7.447 7.421 
       22Alt 6.474 6.493             6.411
       23    7.490 7.489 7.470                             7.411 7.368 7.229            
       23Alt 6.453 6.458 6.462                         6.410                     
       24    7.470 7.468 7.522                                              7.251 7.233 7.242 7.328
3      25    7.505 7.543 7.518 7.467 7.451  7.427 7.345                        
       26    7.590 7.582 7.538                         7.400 7.383 7.376 7.351            
       27    7.570 7.561 7.575                                              7.348 7.283       7.248
       27Alt 7.050 7.019 7.036                                                          6.950   
4      28    7.539 7.541 7.530 7.476 7.431        7.426                        
       28Alt 6.740 6.710 6.751              6.682                           
       29    7.479 7.490 7.474                         7.299 7.260 7.234 7.108            
       30    7.546 7.560 7.522                                              7.331 7.339       7.366          
       30Alt 6.987 6.988 6.950                                                          6.769   
5      31    7.566 7.558 7.557 7.548 7.507        7.491                        
       31Alt 6.900 6.888 6.879              6.800 6.781                        
       32    7.557 7.560 7.545                         7.442 7.412       7.327            
       32Alt 7.130 7.053 7.050                                     6.910               
       33    7.547 7.550 7.532                                              7.392 7.268 7.397   
       33Alt 6.450 6.443 6.451                                                                6.268

Summary Table
Product            6      12     18     24    30    36     42     48     54     60     66    72
Polyurethane Gloss 0.002  0.073  0.058  0.084 0.048 0.072  0.115  0.254  0.236  0.254  0.245 0.155
WB Polyurethane    0.055  0.071  0.095  0.177 0.170 0.187  0.194  0.219  0.221  0.286  0.085 0.321
WB Sanding Sealer  0.061  0.106  0.052  0.111 0.182 0.221  0.247  0.373  0.212  0.204  0.206 0.177
Aqua Deva Metro    0.012  0.053  0.089  0.069 0.112 0.142  0.168  0.227  0.151  0.275  0.146 0.180

Graphs for each product are shown in Figure 2.

*Due to the construction of the floor boards and the location of the impact from the ball, additional baseline readings had to be recorded for certain
areas on the coupons. These values are designated by the coupon number and Alt (alternate).

Product             Slope             Index of Indentation  Rank
                    of Best Fit Line  Resistance           
Polyurethane Gloss  263.41            0.273                  2
WB Polyurethane     217.66            0.331                  3
WB Sander Sealer    205.34            0.351                  4
Aqua Deva Metro     277.07            0.260                  1

The lower the index the less the indentation the better the coating's resistance


Success Rating
A cleanliness study, addressing only various analytical techniques.

Conclusion
Aqua Deva Metro had the lowest Index of Retention, followed by Capitol Polyurethane Gloss.