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Trial Number 1

Trial Purpose:

To evaluate cleaners on second supplied ink.

Date Run:

06/04/2003

Experiment Procedure:

Six products were selected from the previous trial and the SSL's databases based on client supplied information. Even though the substrate to be cleaned was designated as a textile (cloth t-shirts) the initial testing was conducted on a metal substrate so that a quantitative assessment could be made on the selected cleaners. Four of the cleaners were used at full strength, one was used at 20% as recommended by the vendor and the last one was diluted to 10%. The dilutions were made using DI water. All six products were poured into 600 ml glass beakers. All solutions were used at room temperature.

Eighteen preweighed stainless steel coupons were coated with one of the supplied inks, PolysOne Kennesaw Wiflex MX Mixing Colors -blue (85-68-7, 9002-86-2) using a hand held swab and allowed to dry. After drying, coupons were weighed again to determine the amount of ink applied to each coupon. Three coupons were immersed into each solution and cleaned for five minutes using stir-bar agitation. Coupons were rinsed in tap water at 120 F for 15 seconds and dried using a Master Appliance Heat Gun at 500 F for 1 minute. When coupons cooled to room temperature, final weights were measured and product efficiencies were calculated.

Trial Results:

Bio T Max and D-Limonene removed over 80% of the blue ink using immersion cleaning only. The other four products had vast improvement when wiped three times with a paper towel. Of the four, only one did not remove over 90% of the ink. The table below lists the amount of ink added and removed after each cleaning process.

Cleaner Initial wt Final wt % Removed
Bio T Max 0.3850 0.0083 97.84
  0.2028 0.0060 97.04
  0.1178 0.0060 94.91
Graffiti Remover 0.1721 0.4891 -184.20
  0.3962 0.6827 -72.31
  0.2112 0.4958 -134.75
D-Limonene 0.1153 0.0450 60.97
  0.1496 0.0124 91.71
  0.3151 0.0199 93.68
Soy Clear 1500 0.2428 0.0684 71.83
  0.1409 0.0978 30.59
  0.1238 0.1279 -3.31
USA Wash 0.2694 0.2895 -7.46
  0.2340 0.2489 -6.37
  0.2610 0.2776 -6.36
Valtron SP 2201 0.3170 0.3064 3.34
  0.2412 0.2289 5.10
  0.1793 0.1708 4.74
Wipe-Graffiti Remover 0.1721 0.0853 50.44
  0.3962 0.2184 44.88
  0.2112 0.0792 62.50
Wipe-Soy Clear 1500 0.2428 0.0039 98.39
  0.1409 0.0048 96.59
  0.1238 0.0040 96.77
Wipe-USA Wash 0.2694 0.0029 98.92
  0.2340 0.0022 99.06
  0.2610 0.0043 98.35
Wipe-Valtron SP 2201 0.3170 0.0662 79.12
  0.2412 0.0026 98.92
  0.1793 0.0030 98.33

Success Rating:

Results successful using TACT (time, agitation, concentration, and temperature, as well as rinsing and drying) and/or other cleaning chemistries examined.

Conclusion:

The successful cleaners will be evaluated on the next supplied ink.

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