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Trial Purpose:
To reevaluate selected cleaners under heated conditions.
Date Run:
02/01/2000Experiment Procedure:
Eight cleaners were selected from the previous trial. The same six solutions were diluted with DI water to five percent by volume in a 600 ml beaker. The other two products were diluted to 10% as suggested by the vendor. All eight solutions were heated to 130 F on a hot plate. Twenty-four preweighed coupons were coated with the supplied oil and weighed again. Three couponswere cleaned in a solution for five minutes at room temperature using stir-bar agitation. After cleaning the coupons were rinsed for 15 second in tap water at 120 F and allowed to air dry for two hours. Following the drying, final clean weights were recorded and efficiencies were calculated.
SUBSTRATE MATERIAL: Brass Coupons
CONTAMINANTS: Oil-Texaco Lubricant Company Cleartex D (CAS#: 64742-65-0, 68527-02-6)
CONTAMINATING PROCESS USED: Coupons were coated with oil using a hand held swab.
Trial Results:
Heating the solutions improved the cleaning efficiencies for all eight cleaning solutions. Chrisal, SWR Corp, Oakite and Envirosolutions each removed over 90% of the contaminant from the coupons. Table 2 lists the calculated efficiencies for each trial and compares them to the results form Trial 2.
Table 2. Heated Cleaning
Cleaner | Alconox | Chrisal | Savorgran | SWR Corp | Valtech | C&D | Oakite | Envirosolutions |
Coupon 1 | 60.87 | 97.78 | 61.66 | 97.04 | 76.92 | 79.64 | 96.93 | 83.62 |
Coupon 2 | 66.03 | 98.72 | 63.27 | 97.26 | 94.19 | 76.02 | 97.71 | 96.48 |
Coupon 3 | 47.72 | 98.36 | 64.56 | 99.01 | 83.89 | 82.81 | 96.85 | 97.81 |
Average | 58.21 | 98.29 | 63.17 | 97.77 | 85.00 | 79.49 | 97.16 | 92.64 |
Trial 2 | 52.02 | 82.90 | 47.94 | 71.25 | 66.55 | 54.25 | 78.41 | 67.70 |
Success Rating:
A follow up test, usually based on company input.Conclusion:
Heating the solutions improve the removal of the oil from the brass coupons. The solutions with efficiencies over 70% will be evaluated next for removing the rosin solder flux.