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Trial #6

Trial #6

Determining an effective solvent for removing hot-melt adhesive from laminate substrate

33

33

1

66

66

Coupon

06/26/2024

0.00

Immersion/Soak

Alexander Symko

Laminate

Adhesive

None

None

HSPiP

24 strips of laminate were cut such that they were of equal size and were able to fit through the neck of a scintillation vial. Each of these laminate strips were then soiled by melting a single bead of jowatherm 288.60 hot-melt adhesive onto the surface. The coupons were then allowed to soak for 3 hours, with observations being taken every hour. A 1 rating denotes most or complete de-adhesion of the adhesive from the substrate, while a 0 rating means some of or none of the adhesive was de-adhered from the substrate. Once these values were obtained, a HSPiP Solvency sphere was generated to further examine the solubility of the target adhesive.

Solvent 1 Hr 2 Hrs 3 Hrs
Toluene 1 1 1
Dimethyl Carbonate 0 0 0
Xylenes 1 1 1
Benzyl Alcohol 0 0 0
Ethylene Glycol 0 0 0
Methyl Acetate 0 0 0
Undecane 0 0 0
Ethyl Lactate 0 0 0
Acetone 0 1 1
Ethyl Acetate 0 1 1
Methanol 0 0 0
Ethanol 0 0 0
1,3-Dioxolane 1 1 1
Diethyl Carbonate 0 0 1
1-Propanol 0 0 0
Isopropanol 0 0 0
Propylene Carbonate 0 0 0
Thiophene 1 1 1
1-methoxy-2-propanol 0 0 0
Dimethyl Sulfoxide 0 0 0
1-Butanol 0 0 0
Dimethyl Glutarate 0 0 0
Anisole 1 1 1
2-butoxyethyl acetate 0 0 0

HSP Sphere

Conklin HSP Sphere

Toluene, Xylenes, 1,3-Dioxolane, Thiophene, and Anisole were effective at or before the 1 hour mark for de-adhering the adhesive from the laminate. Acetone and Ethyl Acetate were effective at the 2 hour mark, and Diethyl Carbonate was effective at the 3 hour mark. Based on these results, a sphere was generated and the next experiment will utilize solvent blends generated through the solvent optimizer.

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