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Trial #1

Trial #1

Further defining the boundaries of the previously determined HSPiP sphere using a new panel of solvents

36

0

1

3

3

Coupon

03/18/2025

0.00

Immersion/Soak

Alexander Symko

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Pitch

None

None

HSPiP

Eight 20 mL scintillation vials were filled with 15 mL of the selected solvents. Then a fixed amount of shards of hardened pitch were added to each vial and allowed to soak for three hours while being mechanically agitated on a linear roller. For the first hour, observations were taken every 10 minutes to assess any changes in the character of the solution. A zero was denoted as "less than 80% of the pitch had dissolved" while a 1 denoted "more than 80% of the solution dissolved". Dissolution was assessed by visual observation as well as straining of the solvent to examine the size of pitch particulate left in the solution. 

Solvent Final Score
Methyl Benzoate 0
Benzyl Benzoate 0
Tetrahydropyran 0
4-Picoline 1
Cyclohexanone 0
Cyclopentanone 0
Benzaldehyde 1
Butyl Benzoate 0

Based on the results of this experiment, Benzaldehyde and 4-Picoline remain as feasible options to examine for further testing. 

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