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Project #1

Project #1

To determine optimum conditions and materials to clean stainless steel surfaces contaminated with polyurethane.

No

No

No

02/02/1996

John Pastore

Stainless Steel

Simulation of chemical reactor walls and mixing blades. We propose to the use of small stainless steel parts to simulate reactor walls.

Small

Less than 1 lb

Smooth

Hard

Simple

Yes

Adhesive
Coatings

Yes

drumming of product

polymerization of polyurethane

15

1

High Pressure Spray

N Methyl 2 Pyrrolidone

120

120-300

Tap

N-pyrollidone will become a listed chemical. Costs

The reactor must be cleaned of residual polymer solvents and compounding ingredients prior to the start of the next polymerization

MEK, 1 hour

Tap

None

Used Immediately

used for next polymerization

Visual

measure weight of dried polymer removed

The lab found two possible cleaning solutions, Tsquare HTF 85 B and US Polychem 69 MC. Pilot scale testing of the 69 MC yielded inadequate dissolving of the coating. HTF 85 B was as effective as the NMP.

Yes

No

No

No

Yes

Name Class Section
Document Trial #0 Trial 3
Document Trial #1 Trial 3
Document Trial #2 Trial 3
Document Trial #3 Trial 3
Document Trial #4 Trial 3
Document Trial #5 Trial 3
Document Trial #6 Trial 3
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