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Trial Number 3

Trial Purpose:

To evaluate successful products at lower concentration

Date Run:

06/24/2008

Experiment Procedure:

Two products were selected from the previous trial based on successful removal of the resin and had the ability to be diluted. One product was included based on its similarity to a previously tested product which was not dilutable with water. Each of the three products were used at 50% strength in 300 ml glass beakers. Solutions were used at room temperature. Nine preweighed aluminum coupons were coated with the Mereco ECN 809 Base Black resin using a swab. Coupons were weighed a second time to determine the amount of soil added. Three coupons were immersed into each product and cleaned for 20 minutes using no agitation. Following cleaning, coupons were rinsed for 15 seconds in tap water at 68 F and dried using air blow off for 30 seconds at room temperature. Final weights were recorded, and efficiencies were calculated.

Trial Results:

Initial immersion for 20 minutes using the diluted solvents only had marginal success with the Smart Solve 605 working the best at 56.57%. The follow up immersion and single wipe improved the effectiveness of the cleaning solvents, with all three removing more than 85%. The table lists the amount of resin added, the amount remaining and the efficiency for each coupon cleaned using immersion cleaning and the results from the wiping action.

Cleaner Initial wt Final wt % Removed
Smart Solve 605 2.4759 1.5069 39.14
  2.2929 0.8837 61.46
  1.6702 0.5161 69.10
Floor Finish Remover 3.4086 3.0423 10.75
  1.7261 1.0318 40.22
  1.7160 1.2178 29.03
Maxi Solv 3.2685 2.6068 20.24
  2.6387 1.8270 30.76
  2.4476 1.6394 33.02

Additional 5 minute soak with wiping

Cleaner Initial wt Final wt % Removed
Smart Solve 605 1.5069 0.0109 99.28
  0.8837 0.0537 93.92
  0.5161 0.0411 92.04
Floor Finish Remover 3.0423 0.4770 84.32
  1.0318 0.1447 85.98
  1.2178 0.1140 90.64
Maxi Solv 2.6068 0.1178 95.48
  1.8270 0.3517 80.75
  1.6394 0.1857 88.67

Success Rating:

Results suggest a scale-up feasible match for cleaning chemistry and equipment. Pilot plant study with actual parts recommended.

Conclusion:

The same three dilutable products will be tested at longer times without the wipe.

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